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In the analysis of PAs in fruit juice and beer samples, satisfactory recoveries and repeatability were achieved. The intra-day and inter-day precision (relative standard deviations, n = 4, %) at 1.0 and 100.0 μg L −1 spiking concentration were both less than 10%. Under the optimal conditions which were investigated in detail, the limits of detection (LODs, S/N = 3) for PAs in fruit juice were 0.024–0.24 μg L −1, and the related values were 0.011–0.052 μg L −1 for the beer sample. The combination of PIL/MIP-MMF-SPME and high-performance liquid chromatography with diode array detection (HPLC/DAD) was developed for the sensitive determination of phenolic acids (PAs) in fruit juice and beer samples. Under the optimized preparation conditions, the recognition coefficient of PIL-MIP for DBA was as high as 11.6. A PIL, 1-ally-3-vinylimidazolium chloride, was used as a functional monomer, and 3,4-dihydroxybenzenepropanoic acid (DBA) and ethylene dimethacrylate were chosen as the template molecule and cross-linker, respectively, to synthesize the PIL/MIP. In this work, a new molecularly imprinted polymer (MIP) using a poly (ionic liquid) (PIL) as a functional monomer was prepared and utilized as the extraction medium of multiple monolithic fiber solid-phase microextraction (MMF-SPME).
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